本数据集“胺基镱化合物合成工艺数据集”主要面向化学科学领域的合成与纯度表征等研究，包含一类胺基镱化合物（三（N,N-双（三甲基硅基）胺基）镱）的合成工艺开发和表征。该数据集系统整合了研究构建过程中所产生的原始采集数据（生产工艺、表征结果），包括该类胺基镱化合物的研发过程报告和第三方检测CMA报告，为科研人员开展实验复现、结果验证、性能优化提供了完整的数据支撑。胺基镱化合物通过元素分析技术进行了表征，提供了碳、氢、氮等元素的实测值，通过与理论计算值进行对比，确定胺基镱化合物的纯度（＞98%）。
", "ds_source": "元素分析数据测试用德国Elementar Vario EL Cube元素分析仪对其样品进行锻烧，测定碳，氢，氮的含量，平行测试两次，每次2 mg的样品。
", "ds_process_way": "元素分析数据通过计算碳、氢、氮元素含量的实测值总和与理论值总和的比值，确定所合成胺基镱化合物的纯度大于98%。
", "ds_quality": "", "ds_acq_start_time": "2024-07-01 00:00:00", "ds_acq_end_time": null, "ds_acq_place": "", "ds_acq_lon_east": null, "ds_acq_lat_south": null, "ds_acq_lon_west": null, "ds_acq_lat_north": null, "ds_acq_alt_low": null, "ds_acq_alt_high": null, "ds_share_type": "apply-access", "ds_total_size": 3554908, "ds_files_count": 0, "ds_format": "*.pdf", "ds_space_res": "", "ds_time_res": "", "ds_coordinate": "无", "ds_projection": "", "ds_thumbnail": "03fc39ce-2bd9-45ec-80e1-5e88983f67d1.png", "ds_thumb_from": 0, "ds_ref_way": "", "paper_ref_way": "", "ds_ref_instruction": "", "ds_from_station": "", "organization_id": "af683ce0-400b-4f2f-9242-f45f0621e11a", "ds_serv_man": "李红星", "ds_serv_phone": "0931-4967592", "ds_serv_mail": "ncdc@lzb.ac.cn", "doi_value": "", "subject_codes": [ "410" ], "quality_level": 0, "publish_time": "2026-05-20 11:33:16", "last_updated": "2026-05-20 11:33:16", "protected": false, "protected_to": null, "lang": "zh", "cstr": "", "i18n": { "en": { "title": "Ytterbium Amide Compound Synthesis Process Dataset", "ds_format": "pdf", "ds_source": "The elemental analysis data was tested using a German Elementar Vario EL Cube elemental analyzer to calcine the sample and determine the content of carbon, hydrogen, and nitrogen. Two parallel tests were conducted, with 2 mg of the sample each time.
", "ds_quality": "", "ds_ref_way": "", "ds_abstract": "This dataset \"Synthesis Process Dataset of Aminoytterbium Compounds\" is mainly aimed at the research of synthesis and purity characterization in the field of chemical science, including the development and characterization of synthesis processes for a class of aminoytterbium compounds (tris (N, N-bis (trimethylsilyl) amino) ytterbium). This dataset system integrates the raw collected data (production process, characterization results) generated during the research construction process, including the research and development process reports of this type of amino ytterbium compound and third-party detection CMA reports, providing complete data support for researchers to carry out experimental reproduction, result verification, and performance optimization. The amino ytterbium compound was characterized by elemental analysis techniques, providing measured values of carbon, hydrogen, nitrogen, and other elements. By comparing with theoretical calculations, the purity of the amino ytterbium compound was determined to be greater than 98%.
", "ds_time_res": "", "ds_acq_place": "", "ds_space_res": "", "ds_projection": "", "ds_process_way": "The elemental analysis data determines that the purity of the synthesized amino ytterbium compound is greater than 98% by calculating the ratio of the total measured values of carbon, hydrogen, and nitrogen elements to the total theoretical values.
", "ds_ref_instruction": "" } }, "submit_center_id": "ncdc", "data_level": 0, "recommendation_value": 0, "license_type": "https://creativecommons.org/licenses/by/4.0/", "doi_reg_from": "reg_local", "cstr_reg_from": "reg_local", "doi_not_reg_reason": null, "cstr_not_reg_reason": null, "is_paper_in_submitting": false, "ds_topic_tags": [ "稀土", "胺基", "元素分析" ], "ds_subject_tags": [ "工程与技术科学基础学科" ], "ds_class_tags": [], "ds_locus_tags": [], "ds_time_tags": [], "ds_contributors": [ { "true_name": "姚英明", "email": "yaoym@suda.edu.cn", "work_for": "苏州大学", "country": "中国" }, { "true_name": "袁丹", "email": "yuandan@suda.edu.cn", "work_for": "苏州大学", "country": "中国" }, { "true_name": "高伟", "email": "gw@jlu.edu.cn", "work_for": "吉林大学", "country": "中国" } ], "ds_meta_authors": [ { "true_name": "高伟", "email": "gw@jlu.edu.cn", "work_for": "吉林大学", "country": "中国" } ], "ds_managers": [ { "true_name": "高伟", "email": "gw@jlu.edu.cn", "work_for": "吉林大学", "country": "中国" } ], "category": "其他" }