本数据集“胺基钐化合物合成工艺数据集”主要面向化学科学领域的合成与纯度表征等研究，包含一类胺基钐化合物（N,N,N-三（N-三甲基硅甲基亚乙基）胺基钐）的合成工艺开发和表征。该数据集系统整合了研究构建过程中所产生的原始采集数据（生产工艺、表征结果），包括该胺基钐化合物的研发过程报告和第三方检测CMA报告，为科研人员开展实验复现、结果验证、性能优化提供了完整的数据支撑。胺基钐化合物通过元素分析技术进行表征，提供了碳、氢、氮等元素的实测值，通过与理论计算值进行比较，确定胺基钐化合物的纯度（＞98%）。
", "ds_source": "元素分析数据测试用德国Elementar Vario EL Cube元素分析仪对其样品进行锻烧，测定碳，氢，氮的含量，平行测试两次，每次2 mg的样品。
", "ds_process_way": "元素分析数据通过计算碳、氢、氮元素含量的实测值总和与理论值总和的比值，确定所合成胺基钐化合物的纯度大于98%。
", "ds_quality": "", "ds_acq_start_time": "2024-07-01 00:00:00", "ds_acq_end_time": null, "ds_acq_place": "", "ds_acq_lon_east": null, "ds_acq_lat_south": null, "ds_acq_lon_west": null, "ds_acq_lat_north": null, "ds_acq_alt_low": null, "ds_acq_alt_high": null, "ds_share_type": "apply-access", "ds_total_size": 3641345, "ds_files_count": 0, "ds_format": "*.pdf", "ds_space_res": "", "ds_time_res": "", "ds_coordinate": "无", "ds_projection": "", "ds_thumbnail": "6b114780-bc44-4955-85b2-7c5da9c2c94b.png", "ds_thumb_from": 0, "ds_ref_way": "", "paper_ref_way": "", "ds_ref_instruction": "", "ds_from_station": "", "organization_id": "af683ce0-400b-4f2f-9242-f45f0621e11a", "ds_serv_man": "李红星", "ds_serv_phone": "0931-4967592", "ds_serv_mail": "ncdc@lzb.ac.cn", "doi_value": "", "subject_codes": [ "410" ], "quality_level": 0, "publish_time": "2026-05-20 11:45:34", "last_updated": "2026-05-20 11:55:47", "protected": false, "protected_to": null, "lang": "zh", "cstr": "", "i18n": { "en": { "title": "Samarium Amide Compound Synthesis Process Dataset", "ds_format": "*.pdf", "ds_source": "The elemental analysis data was tested using a German Elementar Vario EL Cube elemental analyzer to calcine the sample and determine the content of carbon, hydrogen, and nitrogen. Two parallel tests were conducted, with 2 mg of the sample each time.
", "ds_quality": "", "ds_ref_way": "", "ds_abstract": "This dataset \"Synthesis Process Dataset of Amine Samarium Compounds\" is mainly aimed at the research of synthesis and purity characterization in the field of chemical science, including the development and characterization of synthesis processes for a class of amine samarium compounds (N, N, N-tris (N-trimethylsilmethylethylene) amine samarium). This dataset system integrates the raw collected data (production process, characterization results) generated during the research construction process, including the research and development process report of the amino samarium compound and the third-party detection CMA report, providing complete data support for researchers to carry out experimental reproduction, result verification, and performance optimization. Amino samarium compounds are characterized using elemental analysis techniques, providing measured values of carbon, hydrogen, nitrogen, and other elements. By comparing these values with theoretical calculations, the purity of amino samarium compounds (>98%) is determined.
", "ds_time_res": "", "ds_acq_place": "", "ds_space_res": "", "ds_projection": "", "ds_process_way": "The elemental analysis data determines that the purity of the synthesized amino samarium compound is greater than 98% by calculating the ratio of the total measured values of carbon, hydrogen, and nitrogen elements to the total theoretical values.
", "ds_ref_instruction": "" } }, "submit_center_id": "ncdc", "data_level": 0, "recommendation_value": 0, "license_type": "https://creativecommons.org/licenses/by/4.0/", "doi_reg_from": "reg_local", "cstr_reg_from": "reg_local", "doi_not_reg_reason": null, "cstr_not_reg_reason": null, "is_paper_in_submitting": false, "ds_topic_tags": [ "稀土", "胺基", "元素分析" ], "ds_subject_tags": [ "工程与技术科学基础学科" ], "ds_class_tags": [], "ds_locus_tags": [], "ds_time_tags": [], "ds_contributors": [ { "true_name": "姚英明", "email": "yaoym@suda.edu.cn", "work_for": "苏州大学", "country": "中国" }, { "true_name": "袁丹", "email": "yuandan@suda.edu.cn", "work_for": "苏州大学", "country": "中国" }, { "true_name": "高伟", "email": "gw@jlu.edu.cn", "work_for": "吉林大学", "country": "中国" } ], "ds_meta_authors": [ { "true_name": "高伟", "email": "gw@jlu.edu.cn", "work_for": "吉林大学", "country": "中国" } ], "ds_managers": [ { "true_name": "高伟", "email": "gw@jlu.edu.cn", "work_for": "吉林大学", "country": "中国" } ], "category": "其他" }