To determine the stratigraphic affiliation of quartz sandstone in the Liaodong Bay area of the Bohai Sea, as well as the source characteristics and geological significance of this set of quartz sandstone, quartz sandstone samples obtained near 2482 meters of the BD4-1a well in Liaodong Bay were analyzed and studied. The samples were numbered 2482-1, 2482-2, 2482-3, 2482-4, and 2482-5, respectively. Whole rock geochemical analysis was conducted on five samples, and zircon U-Pb dating was conducted on sample 2482-3, obtaining 135 zircon ages
| collect time | 2016/05/01 - 2016/08/01 |
|---|---|
| collect place | Near 2482m of BD4-1a well in the Liaodong Bay area of Bohai Sea |
| data size | 117.0 KiB |
| data format | docx |
| Coordinate system |
Data source: Element composition data comes from the following literature: [1] Zhao Zilin, Zhou Xuewei, Li Kuizhou, Guo Tao, Peng Jingsong, Hou Mingcai. Source characteristics and geological significance of quartz sandstone in the Changlongshan Formation of the Neoproterozoic in the Liaodong Bay area [J/OL]. Journal of Sedimentology https://doi.org/10.14027/j.issn.1000-0550.2022.093 Testing instruments, methods, and processes: (1) Whole rock geochemistry The main and trace element analysis of the entire rock was completed by Wuhan Shangpu Analysis Technology Co., Ltd. The main elements of the entire rock were tested using a Japanese physics Primus II X-ray fluorescence spectrometer (XRF), and the sample was dried at 105 ℃ before weighing~1.0 g to calculate the loss on ignition; Glass sheets were made using anhydrous Li2B4O7 as the flux and NH4NO3 as the oxidant for XRF testing. The trace element testing of the entire rock was completed using an inductively coupled plasma mass spectrometer Agilent 7700e ICP-MS analysis. A weighed 50 mg sample powder was placed in a Teflon dissolution bomb, followed by the addition of HF and HNO3. The sample was then heated in an oven at~190 ℃ for more than 24 hours to achieve complete dissolution; Use 1 mL of internal standard In (concentration 1 × 10-6) Re processing; Finally, transfer the solution into a polyethylene bottle and dilute it to 100 g with 2% HNO3 before conducting ICP-MS testing. (2) Zircon U-Pb age The selection, target making, and CL photography of zircons were completed at Nanjing Hongchuang Geological Exploration Technology Service Co., Ltd. Firstly, stick double-sided adhesive tape onto the glass slide, gently shake off the sorted zircon particles to a low magnification microscope, and use a very fine hook to neatly and orderly stick the particles onto the double-sided adhesive tape (sedimentary rocks generally stick 150-200 particles, igneous rocks stick 50-100 particles), with a diameter of 1cm × A 1cm circular hollow tube is pasted onto a glass slide and the particles are kept at the center. The prepared epoxy resin is poured and placed in a constant temperature oven for two days. After solidification, the zircon target is roughly ground, finely ground, and polished. Subsequently, a cathodoluminescence (CL) micrograph was taken after carbon spraying on the surface, and images of reflected and transmitted light were collected under a regular microscope. After collecting the images, use drawing software to concatenate them, and compare the three types of images together to select a better measurement point position. U-Pb dating was completed in the State Key Laboratory of Oil and Gas Reservoir Geology and Development Engineering (Chengdu University of Technology), and the experimental equipment was the Resolution LR 193nm laser ablation system of American Applied Spectrum Company and Agilent 7900 mass spectrometer. In this analysis, the laser energy density was 3.5 J/cm2, the beam spot diameter was 29 µ m, the frequency was 8 Hz, and the erosion lasted for 45 seconds; Using standard zircon 91500 as the external standard to correct instrument quality discrimination and elemental fractionation; Using standard zircon PLE as a blind standard to test data quality; Use NIST SRM610 as the external standard and Si as the internal standard to calibrate the trace element content of zircon. The offline processing of analytical data is completed using software ICPMSDataCal. Utilizing Isoplot/Ex_ Plot the U-Pb age harmony map and calculate the age weighted average of zircon samples using ver3
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| # | number | name | type |
| 1 | 40200-02021301 | Material basis for hydrocarbon accumulation | other |
| 2 | 42102141 | Sedimentary sequence and provenance analysis of the Liantuo Formationin Dahongshan area, northern Yangtze Block | National Natural Science Foundation of China |
| 3 | 2022T150076 | China Postdoctoral Science Foundation Project | other |
| 4 | CCL2014TIXZSS0870 | Petroleum Geological Characteristics of Buried Hills in Bohai Sea, Accumulation Mechanism of Typical Oil and Gas Reservoirs and Prediction of Favorable Exploration Zones | other |
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| # | title | file size |
|---|---|---|
| 1 | _ncdc_meta_.json | 7.7 KiB |
| 2 | 赵子霖附表.docx | 117.0 KiB |
Liaodong Bay Neoproterozoic Changlongshan Formation quartz sandstone geochemistry clastic zircon U-Pb age
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