A report on the production process research and development of 8 types and 20 high-purity chiral rare earth organic complexes was provided. Including:
Small scale experiments and 10 gram scale synthesis of chiral pyridine bis imidazoline rare earth complexes (5 types)
Small scale experiments and 10 gram scale synthesis of chiral pyridine bisoxazoline rare earth complexes (4 types)
Small scale experiments and 10 gram scale synthesis of 3 chiral cyclohexanediamine Salen rare earth complexes (2 types)
Small scale experiments and 10 gram level synthesis of 4-chiral naphthalene dioxy phosphate rare earth complexes (2 types)
Small scale experiments and 10 gram level synthesis of 5 chiral phenyl oxazoline rare earth complexes (2 types)
Small scale experiment and 10 gram level synthesis of rare earth complexes with 6-chiral ortho phenanthroline and oxazoline (1 type)
Small scale experiments and 10 gram level synthesis of 7 chiral Schiff base rare earth complexes (2 types)
Small scale experiments and 10 gram level synthesis of rare earth complexes with dual proline esters based on 8-chiral phenolic frameworks (2 types)
Meet the preparation needs of high-end chiral rare earth reagents in the scientific research field, and support the high-value and multifunctional application of rare earth strategic resources in the field of scientific research reagents.
This resource comes from the ten gram level synthesis research process of chiral rare earth organic complexes, and the relevant data was collected from the Synthesis Laboratory of Beijing University of Chemical Technology. Collect the feeding amount of reactants and the yield of products using a high-precision balance (accurate to 0.001 grams), and calculate the production rate. By strictly regulating the synthesis experiment process and verifying it multiple times with multiple people, the reliability of data collection is ensured. The structure and purity of the product were verified by methods such as nuclear magnetic resonance spectroscopy, elemental analysis, and chiral HPLC testing.
This resource processing method is based on multiple organic synthesis processes and results. By providing a detailed description of the organic synthesis process operation, recording the data of the organic synthesis process in detail, and conducting multiple verification experiments, a production process document for high-purity chiral rare earth organic complexes has been compiled.
This resource comes from the ten gram level synthesis research process of chiral rare earth organic complexes, and the relevant data was collected from the Synthesis Laboratory of Beijing University of Chemical Technology. Collect the feeding amount of reactants and the yield of products using a high-precision balance (accurate to 0.001 grams), and calculate the production rate. By strictly regulating the synthesis experiment process and verifying it multiple times with multiple people, the reliability of data collection is ensured.
| # | number | name | type |
| 1 | 2022YFF0709800 | Development of High-Purity Rare Earth Reagents and Analytical Techniques | National key R & D plan |
| 2 | 2022YFF0709803 | Development and application of reagent synthesis technology for high-purity chiral rare earth organic complexes |
This work is licensed under
CC BY 4.0 (Creative Commons Attribution 4.0 International License).
CSTR:11738.11.ncdc.gcxtsj.db7373.2026
10.12072/ncdc.gcxtsj.db7373.2026
